Carbon/silica hybrid aerogels with controlled porosity by a quick one-pot synthesis

نویسندگان

چکیده

Hybrid aerogels from carbon and silica precursors were obtained via a rapid process by microwave heating the use of catalysts. Due to varied nature precursors, one key points in synthesizing these hybrid is ensure homogeneous mixture during entire synthesis process. It well known that using microwaves may accelerate some reactions, but our study also evaluated so-called effect on certain reactions. Another strategy boost polymerization reactions addition specific catalyst. The small amount aminosilanes precursor solution was with excellent results. combination two different strategies (i.e., aminosilanes) makes it possible obtain define final porous properties usual variables (e.g., dilution ratio) sol-gel synthesis.

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

High porosity polyethylene aerogels

Monolithic aerogels of high molecular weight polyethylene (Mw= 3x106- 6x106 g/mol) have been prepared by solvent extraction with supercritical carbon dioxide from thermoreversible gels prepared in decalin. These low density and highly porous aerogels present an apparent porosity up to 90%. The aerogel morphology observed by scanning electron microscopy (SEM) is characterized by spherulitic stru...

متن کامل

One-pot synthesis of Fe3O4 nanoprisms with controlled electrochemical properties.

Fe(3)O(4) nanoprisms, synthesized by a solvothermal process, exhibited crystal plane dependent electrochemical activities, which opens an approach to nanoscale materials with controlled electrochemical properties.

متن کامل

A Modified-One Pot Synthesis of Diaminoglyoxime

The one pot reaction of glyoxal and hydroxylamine hydrochloride in aqueous sodium hydroxide was found to be a safe and inexpensive method for the preparation of diaminoglyoxime. By increasing stoichiometric ratio of the hydroxylamine hydrochloride and decreasing the solvent volume, the product yield increased considerably (~ 70%).

متن کامل

One-pot synthesis of responsive catalytic Au@PVP hybrid nanogels.

Responsive catalytic hybrid nanogels with Au nanoparticle cores and a polyvinylpyrrolidone (PVP) based gel shell are prepared through a novel one-pot approach. The embedded Au nanoparticles demonstrate both a pH-modulated catalytic activity and anti-aggregation properties upon recycling.

متن کامل

One-Pot Synthesis of Hybrid Conjugated Oligomer-Ag Nanoparticles

Here we report one-pot, straightforward synthesis of hybrid conjugated oligomer-silver nanoparticles (AgNPs) by utilizing tertiary alkyl amine and fluorenebenzothiodiazole-containing conjugated oligomer that both acts as a reducing agent in the reduction of silver ions into metallic silver and as a matrix to accommodate the newly formed AgNPs. By tuning the reaction conditions, it is possible t...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ژورنال

عنوان ژورنال: Journal of Non-crystalline Solids

سال: 2021

ISSN: ['1873-4812', '0022-3093']

DOI: https://doi.org/10.1016/j.jnoncrysol.2021.120992